目錄
前言
Chapter 1 Introduction
1.1 Significance of Chemical Experiments
1.2 Teaching Objectives of Inorganic Chemistry Experiment Course
1.3 Requirements and Methods of Experiment Course
Chapter 2 Basic Knowledge of the Lab
2.1 Laboratory Safety Knowledge, Discipline and Precautions
2.2 The Use, Cleaning and Drying of Inorganic Chemical Apparatuses
2.3 Introduction and Use of Commonly Used Heating Equipment
2.4 General Knowledge of Chemical Reagents
Chapter 3 Basic Inorganic Chemistry Experiments
Exp.1 Receiving, Washing and Drying the Apparatuses
Exp.2 Transferring Chemical Reagents and Operating Test Tubes
Exp.3 Preparation of Solutions
Exp.4 Determination of the Molecular Weight of CO
Exp.5 Determination of Crystal Water Content in Blue Vitriol
Exp.6 Purification and Qualitative Test of Crude Salt
Exp.7 Determination of the Degree of Dissociation and Dissociation Constant of Acetic Acid
Exp.8 Qualitative Identification of Some Essential Elements in Organisms
Exp.9 Determination of the Solubility Product of PbI
Exp.10 Determination of Chemical Reaction Rate and Activation Energy
Exp.11 Preparation of Potassium Permanganate by Solid Alkali Fusion Oxidation Method
Exp.12 Preparation of Ammonium Ferrous Sulfate Crystals
Exp.13 Purification and Solubility Determination of Potassium Nitrate
Exp.14 Oxidation-reduction Reaction and Equilibrium
Chapter 4 Elemental Inorganic Chemistry Experiments
Exp.15 s-Block Elements (Alkali Metals and Alkaline Earth Metals)
Exp.16 p-Block Nonmetallic Elements (Ⅰ) (Halogen, O, S)
Exp.17 p-Block Nonmetallic Elements (Ⅱ) (N, P, C, Si, B)
Exp.18 p-Block Metallic Elements (Al, Sn, Pb, Sb, Bi)
Exp.19 Properties of Element Compounds in the d-Block (Ⅰ)
Exp.20 Properties of Element Compounds in the d-Block (Ⅱ)
Exp.21 ds-Block Metals (Cu, Ag, Zn, Cd, Hg)
Exp.22 Separation and Identification of Unknown Cations
Exp.23 Separation and Identification of Unknown Anions
Chapter 5 Comprehensive and Design Experiments
Exp.24 Preparation and Composition Measurement of a Cobalt (Ⅲ) Complex
Exp.25 Preparation and Component Analysis of the Large Crystal of Cuprammonium Sulfate (Ⅱ)
Exp.26 Preparation and Quality Analysis of Zinc Gluconate
Exp.27 Preparation and Photocatalytic Performance of Titanium Dioxide Nanoparticles
Exp.28 Preparation of Zinc Vitriol
Exp.29 Preparation and Composition Analysis of Potassium Bis (oxalato) Copper (Ⅱ) Dihydrate
Exp.30 Synthesis and Composition Analysis of Potassium Trioxalatoferrate (Ⅲ)
Exp.31 Preparation and Content Analysis of Calcium Peroxide
Exp.32 Preparation of Basic Copper Carbonate
Exp.33 Determination of the Composition and Stability Constant of Titanium (Ⅳ) Peroxide Complex
Exp.34 Preparation and Content Analysis of Cobalt Ferrite CoFe2O
Exp.35 Preparation, Optical Absorption Properties and Stability
Exp.37 Preparation and Application of Na2S2O
Exp.38 Home-made Plant Acid-base Indicator
Exp.39 Qualitative Identification of Iodine in Kelp and Salt
Exp.40 Interesting Chemical Experiment (Ⅰ)
Exp.41 Interesting Chemical Experiment (Ⅱ)
Exp.42 Identification of Salt and Sodium Nitrite
第1章 緒論
1.1 化學實驗的重要意義
1.2 無機化學實驗課的教學目的
1.3 實驗課的學習要求和方法
第2章 實驗室基礎知識
2.1 實驗室安全知識、紀律及注意事項
2.2 無機化學常用儀器的使用、洗滌與乾燥
2.3 常用加熱器具的介紹與使用
2.4 化學試劑的一般知識
第3章 基礎無機化學實驗
實驗1 儀器的認領、洗滌與乾燥
實驗2 試劑的取用和試管操作
實驗3 溶液的配製
實驗4 二氧化碳分子量的測定
實驗5 膽礬結晶水的測定
實驗6 粗鹽的提純與定性檢驗
實驗7 乙酸解離度和解離常數的測定
實驗8 生物體中幾種必需元素的定性鑒定
實驗9 碘化鉛溶度積的測定
實驗10 化學反應速率與活化能的測定
實驗11 固體鹼熔氧化法製備高錳酸鉀
實驗12 硫酸亞鐵銨晶體的製備
實驗13 硝酸鉀提純和溶解度測定
實驗14 氧化還原反應及平衡
第4章 元素無機化學實驗
實驗15 s區元素(鹼金屬、鹼土金屬)
實驗16 p區非金屬元素(一)(鹵素、氧、硫)
實驗17 p區非金屬元素(二)(氮、磷、碳、硅、硼)
實驗18 p區金屬元素(鋁、錫、鉛、銻、鉍)
實驗19 d區元素化合物的性質(一)
實驗20 d區元素化合物的性質(二)
實驗21 ds區金屬(銅、銀、鋅、鎘、汞)
實驗22 未知陽離子的分離與鑒定
實驗23 未知陰離子的分離與鑒定
第5章 綜合與設計實驗
實驗24 一種鈷(Ⅲ)配合物的製備與組成測定
實驗25 硫酸四氨合銅(Ⅱ)大晶體的製備及組成分析
實驗26 葡萄糖酸鋅的製備與質量分析
實驗27 納米二氧化鈦的製備和光催化性能
實驗28 七水合硫酸鋅的製備
實驗29 二水合二草酸根合銅(Ⅱ)酸鉀的製備與組成分析
實驗30 三草酸根合鐵(Ⅲ)酸鉀的合成及組成分析
實驗31 過氧化鈣的製備及含量分析
實驗32 鹼式碳酸銅的製備
實驗33 過氧化氫合鈦(Ⅳ)配合物的組成和穩定常數的測定
實驗34 鈷鐵氧體CoFe2O4的製備及含量分析
實驗35 金(銀)膠體的製備、光學吸收性質和穩定性
實驗36 金屬離子與血清白蛋白的相互作用
第6章 生活中的化學
實驗37 硫代硫酸鈉的製備和應用
實驗38 自製植物酸鹼指示劑
實驗39 海帶和食鹽中碘的定性鑒定
實驗40 化學趣味實驗(一)
實驗41 化學趣味實驗(二)
實驗42 食鹽和亞硝酸鈉的鑒別