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有機化學實驗(英漢雙語教材高等學校十二五規劃教材)

  • 作者:編者:陳彪//魏永慧
  • 出版社:化學工業
  • ISBN:9787122173140
  • 出版日期:2019/08/01
  • 裝幀:平裝
  • 頁數:211
人民幣:RMB 36 元      售價:
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內容大鋼
    本書是編者在總結多年來有機化學實驗的教學經驗及近年來實施雙語教學實踐的基礎上,參考了國內外出版的同類教材,採用英漢兩種語言,編寫的與有機化學雙語課程配套使用的《有機化學實驗》教材。
    全書包括:有機化學實驗的一般知識,有機化學實驗的基礎知識和基本操作,有機化學綜合實驗(包括合成及分離提取兩大部分),附錄及參考文獻。
    本書可使學生在掌握有機化學實驗基本原理、基本技能的同時,提高英語實際應用能力和水平,適用於化學、醫學、藥學及相關專業的學生使用,也可作為有機化學及相關專業碩士研究生的實驗參考書。

作者介紹
編者:陳彪//魏永慧

目錄
Chapter 1  Introduction of Experimental Organic Chemistry
  1.1  Basic Rules for the Organic Chemistry Lab
  1.2  Common Lab Equipment and Apparatus
  1.3  General Lab Safety
  1.4  Disposal of Lab Waste
  1.5  Common Organic Solvents
  1.6  Experimental Preview Record and Laboratory Report
  1.7  Chemical Literature
  Reference
Chapter 2  Basic Experimental Techniques
  2.1  Heating and Cooling
  2.2  Drying and Drying Agent
  2.3  Filtration
  2.4  Solvent Extraction and Solution Washing
  2.5  The Purification and Separation of Liquid Organic Substances
  2.6  The Purification and Separation of Solid Organic Substances
  2.7  Chromatographic Techniques
  2.8  The Determination of the Physical Constant of Organic Compound
Chapter 3  Comprehensive Experiment
  Part 1  Synthesis
    3.1  Synthesis of Cyclohexene
    3.2  Synthesis of Ethyl Bromide
    3.3  Synthesis of 2-chlorobutane (sec-butyl chloride)
    3.4  Synthesis of diethyl ether
    3.5  Synthesis of Phenetole (ethyl phenolate)
    3.6  Synthesis of Benzoic Acid and Benzyl Alcohol
    3.7  Synthesis of Acetophenone
    3.8  Synthesis of Benzophenone (Friedel- Crafts aeylation method)
    3.9  Synthesis of Cyclohexanone
    3.10  Synthesis of Adipie Acid
    3.11  Synthesis of Benzoic Acid
    3.12  Synthesis of Cinnamic Acid
    3.13  Synthesis of Ethyl Acetate
    3.14  Synthesis of Isoamyl Acetate (banana oil)
    3.15  Synthesis of Acetylsalicylic Acid (aspirin)
    3.16  Synthesis of Methyl Salicylate (oil of wintergreen)
    3.17  Synthesis of Ethyl Aeetoacetate
    3.18  Synthesis of Acetanilide
    3.19  Synthesis of p-toluidine
    3.20  Synthesis of Anthranilic Acid (2-aminobenzoic acid)
    3.21  Synthesis of Phenoxyacetic Acid
    3.22  Synthesis of Methyl Orange
    3.23  Synthesis of Benzocaine
    3.24  Synthesis of N-acetyl-p-toluidine
    3.25  Synthesis of Benzoin
    3.26  Synthesis of 2-Nitroresorcinol
    3.27  Synthesis of Quinoline
    3.28  Synthesis of Nikethamide
    3.29  The Reduction of Camphor  i
    3.30  Synthesis of a-(2,5-xylyloxyl) Propyl Chloride and Monitoration of Reaction Process

  Part 2  Extraction and Separation  i
    3.31  The Recrystallization of Benzoic Acid
    3.32  Extraction and Purification of Nicotine
    3.33  Isolation of Caffeine From Tea Leave
    3.34  Isolation of Effective Components from the Citrus
    3.35  Isolation of Benberine from Coptis chinensis Franch
    3.36  Paper Chromatography of Amino Acid
    3.37  Paper Electrophoresis of Amino Acid
    3.38  Separation of Green Leaf Pigments by TLC
Chapter 4  Appendix
  4.1  Experiments from the Literature
  4.2  List of the Elements with Their Symbols and Atomic Masses
  4.3  Main Families of Organic Compounds
  4.4  Boling Point and Density of Some Common Organic Reagents
第1章  有機化學實驗基礎知識
  1.1  有機化學實驗的基本規則
  1.2  常用的玻璃儀器和實驗裝置
  1.3  有機化學實驗的安全知識
  1.4  有機化學實驗廢物的處置
  1.5  常用有機溶劑及純化
  1.6  實驗預習記錄和實驗報告
  1.7  有機化學的文獻資料
第2章  有機化學實驗基本操作
  2.1  加熱和冷卻
  2.2  乾燥與乾燥劑
  2.3  過濾
  2.4  萃取和洗滌
  2.5  液體有機化合物的分離與純化
  2.6  固體有機化合物的提純
  2.7  色譜法
  2.8  有機化合物物理常數的測定
第3章  綜合實驗
  第一部  分製備
    3.1  環己烯的製備
    3.2  溴乙烷的製備
    3.3  2-氯丁烷的製備
    3.4  乙醚的製備
    3.5  苯乙醚的製備
    3.6  苯甲醇和苯甲酸的製備
    3.7  苯乙酮的製備
    3.8  二苯甲酮(?基化法)的製備
    3.9  環己酮的製備
    3.10  己二酸的製備
    3.11  苯甲酸的製備
    3.12  肉桂酸的製備
    3.13  乙酸乙酯的製備
    3.14  乙酸異戊酯的製備(香蕉油)
    3.15  乙?水楊酸的製備(阿司匹林)
    3.16  水楊酸甲酯的製備(冬青油)
    3.17  乙?乙酸乙酯的製備

    3.18  乙?苯胺的製備
    3.19  對甲苯胺的合成
    3.20  鄰氨基苯甲酸的合成
    3.21  苯氧乙酸的製備
    3.22  甲基橙的製備
    3.23  苯佐卡因的製備
    3.24  對甲基-N-乙?苯胺的合成
    3.25  安息香的合成
    3.26  2-硝基雷瑣酚的製備
    3.27  ??的製備
    3.28  尼可剎米的製備
    3.29  樟腦的還原反應
    3.30  降血脂葯吉非貝齊中間體3-(2,5-二甲基苯氧基)-1-氯丙烷的製備
  第二部分  提取、分離與鑒定
    3.31  苯甲酸的提純
    3.32  煙鹼的提取與鑒定
    3.33  從茶葉中提取咖啡因
    3.34  橘皮中有效成分的提取、分離與鑒定
    3.35  黃連中黃連素的提取及鑒定
    3.36  紙色譜分離鑒定氨基酸
    3.37  紙上電泳分離鑒定氨基酸
    3.38  薄層色譜法分離葉綠素
參考文獻

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