Chapter 1 Introduction of Experimental Organic Chemistry 1.1 Basic Rules for the Organic Chemistry Lab 1.2 Common Lab Equipment and Apparatus 1.3 General Lab Safety 1.4 Disposal of Lab Waste 1.5 Common Organic Solvents 1.6 Experimental Preview Record and Laboratory Report 1.7 Chemical Literature Reference Chapter 2 Basic Experimental Techniques 2.1 Heating and Cooling 2.2 Drying and Drying Agent 2.3 Filtration 2.4 Solvent Extraction and Solution Washing 2.5 The Purification and Separation of Liquid Organic Substances 2.6 The Purification and Separation of Solid Organic Substances 2.7 Chromatographic Techniques 2.8 The Determination of the Physical Constant of Organic Compound Chapter 3 Comprehensive Experiment Part 1 Synthesis 3.1 Synthesis of Cyclohexene 3.2 Synthesis of Ethyl Bromide 3.3 Synthesis of 2-chlorobutane (sec-butyl chloride) 3.4 Synthesis of diethyl ether 3.5 Synthesis of Phenetole (ethyl phenolate) 3.6 Synthesis of Benzoic Acid and Benzyl Alcohol 3.7 Synthesis of Acetophenone 3.8 Synthesis of Benzophenone (Friedel- Crafts aeylation method) 3.9 Synthesis of Cyclohexanone 3.10 Synthesis of Adipie Acid 3.11 Synthesis of Benzoic Acid 3.12 Synthesis of Cinnamic Acid 3.13 Synthesis of Ethyl Acetate 3.14 Synthesis of Isoamyl Acetate (banana oil) 3.15 Synthesis of Acetylsalicylic Acid (aspirin) 3.16 Synthesis of Methyl Salicylate (oil of wintergreen) 3.17 Synthesis of Ethyl Aeetoacetate 3.18 Synthesis of Acetanilide 3.19 Synthesis of p-toluidine 3.20 Synthesis of Anthranilic Acid (2-aminobenzoic acid) 3.21 Synthesis of Phenoxyacetic Acid 3.22 Synthesis of Methyl Orange 3.23 Synthesis of Benzocaine 3.24 Synthesis of N-acetyl-p-toluidine 3.25 Synthesis of Benzoin 3.26 Synthesis of 2-Nitroresorcinol 3.27 Synthesis of Quinoline 3.28 Synthesis of Nikethamide 3.29 The Reduction of Camphor i 3.30 Synthesis of a-(2,5-xylyloxyl) Propyl Chloride and Monitoration of Reaction Process
Part 2 Extraction and Separation i 3.31 The Recrystallization of Benzoic Acid 3.32 Extraction and Purification of Nicotine 3.33 Isolation of Caffeine From Tea Leave 3.34 Isolation of Effective Components from the Citrus 3.35 Isolation of Benberine from Coptis chinensis Franch 3.36 Paper Chromatography of Amino Acid 3.37 Paper Electrophoresis of Amino Acid 3.38 Separation of Green Leaf Pigments by TLC Chapter 4 Appendix 4.1 Experiments from the Literature 4.2 List of the Elements with Their Symbols and Atomic Masses 4.3 Main Families of Organic Compounds 4.4 Boling Point and Density of Some Common Organic Reagents 第1章 有機化學實驗基礎知識 1.1 有機化學實驗的基本規則 1.2 常用的玻璃儀器和實驗裝置 1.3 有機化學實驗的安全知識 1.4 有機化學實驗廢物的處置 1.5 常用有機溶劑及純化 1.6 實驗預習記錄和實驗報告 1.7 有機化學的文獻資料 第2章 有機化學實驗基本操作 2.1 加熱和冷卻 2.2 乾燥與乾燥劑 2.3 過濾 2.4 萃取和洗滌 2.5 液體有機化合物的分離與純化 2.6 固體有機化合物的提純 2.7 色譜法 2.8 有機化合物物理常數的測定 第3章 綜合實驗 第一部 分製備 3.1 環己烯的製備 3.2 溴乙烷的製備 3.3 2-氯丁烷的製備 3.4 乙醚的製備 3.5 苯乙醚的製備 3.6 苯甲醇和苯甲酸的製備 3.7 苯乙酮的製備 3.8 二苯甲酮(?基化法)的製備 3.9 環己酮的製備 3.10 己二酸的製備 3.11 苯甲酸的製備 3.12 肉桂酸的製備 3.13 乙酸乙酯的製備 3.14 乙酸異戊酯的製備(香蕉油) 3.15 乙?水楊酸的製備(阿司匹林) 3.16 水楊酸甲酯的製備(冬青油) 3.17 乙?乙酸乙酯的製備